4-Bromothiophenol → HCID 54525745, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([SH:8])=[CH:4][CH:3]=1.Br[CH2:10][C:11]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])=[O:12]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH2:10][C:11]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])=[O:12])=[CH:4][CH:3]=1Participants
3
Procedure
The subject compound was prepared starting from 4-bromobenzenethiol and t-butyl bromoacetate in the same manner as Reference example 6-1.
Workup
- customThe subject compound was prepared
Sources & evidence
- ORD record
- ord-c84fb6519206413f947f94cad044f102
- Source dataset
- uspto-grants-2007_05
- Patent number
- US07220773B2
Reaction notes
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