反应详情

To a stirring solution of 3-phenoxyaniline (185 mg, 1.0 mmol) in acetone (4.0 mL) at 0° C. was added thiophosgene (0.23 mL, 3.0 mmol) and the resulting reaction maintained for 30 min. The reaction determined complete by TLC (4:1 hexane/EtOAc). The reaction was concentrated, azeotroped with toluene and taken on without further purification.

1. customthe resulting reaction
2. temperaturemaintained for 30 min
3. concentrationThe reaction was concentrated
4. customazeotroped with toluene
5. customtaken on without further purification