Caprolactam → HCID 86610174, compound

HRID 1353135Notes

Reaction equation

HRID 1353135 reaction equation
[C:1]1(=[O:8])[NH:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[F:9][B-:10]([F:13])([F:12])[F:11].[H+]>>[F:9][B-:10]([F:13])([F:12])[F:11].[C:1]1(=[O:8])[NH:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 7768CaprolactamHCID 28118Tetrafluoroboric acid

Product 1

HCID 86610174HCID 86610174, compound

Procedure

The procedure is the same as in example 2 except that the amount of ε-caprolactam and tetrafluoroboric acid added is increased to 1 mol respectively. Desired product of caprolactam tetrafluoroborate was obtained with a yield of 96.3%. No melting point was observed. The density, the viscosity, the ionic conductivity, the glass transition temperature, and the Hammett acidic scale H0 are the same as those of in example 2.

Workup

  1. additionadded
  2. temperatureis increased to 1 mol respectively

Sources & evidence

ORD record
ord-88a6c0e695924b01a09452025f4ed1df
Source dataset
uspto-grants-2007_05
Patent number
US07220869B2

Reaction notes

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