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4-Ethylphenethylamine → 3-(3-{[2-(4-Ethyl-phenyl)-ethylcarbamoyl]-methoxy}-phenyl)-2-methoxy-propionic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Ethylphenethylamine | HCID 144047 | — |
| 反応物 | (2S,1R)-2-ethoxy-3-(4-{1-[2-(4-phenoxy-phenyl)-ethylcarbamoyl]-ethoxy}-phenyl)propionic acid | HCID 9847886 | — |
| 反応物 | 3-(3-Carboxymethoxy-phenyl)-2-methoxy-propionic acid methyl ester | HCID 58646610 | — |
| 生成物 | 3-(3-{[2-(4-Ethyl-phenyl)-ethylcarbamoyl]-methoxy}-phenyl)-2-methoxy-propionic acid | HCID 23132766 | — |
反応手順
The title compound was prepared from 3-(3-carboxymethoxy-phenyl)-2-methoxy-propionic acid methyl ester (PREPARATION 4, step 2) and 2-(4-ethyl-phenyl)-ethylamine via the same procedure used for the preparation of (2S,1R)-2-ethoxy-3-(4-{1-[2-(4-phenoxy-phenyl)-ethylcarbamoyl]-ethoxy}-phenyl)-propionic acid (Example 1, step 3) to produce a colorless oil. MS (ES) for C22H27NO5 [M+H]+: 386.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07220880B2 |
| 出典データセット | uspto-grants-2007_05 |
| ORD ID | ord-6ae119d3c44745ffa79f37b21854852a |
| 出典メモ | uspto-grants-2007_05 |