HuagongsheHuagongshe Chemistry Print Report · For research reference only
DL-Phenylalanine, methyl ester → HCID 69417998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | DL-Phenylalanine, methyl ester | HCID 75737 | — |
| Reactant | (2S,1R)-2-ethoxy-3-(4-{1-[2-(4-phenoxy-phenyl)-ethylcarbamoyl]-ethoxy}-phenyl)propionic acid | HCID 9847886 | — |
| Reactant | (2S)-3-(4-carboxymethoxy-phenyl)-2-methoxy-propionic acid ethyl ester | HCID 58864673 | — |
| Product | HCID 69417998 | HCID 69417998 | — |
Reaction Steps
The title compound was prepared from (2S)-3-(4-carboxymethoxy-phenyl)-2-methoxy-propionic acid ethyl ester (PREPARATION 3, step 2) and 2-amino-3-phenyl-propionic acid methyl ester via the same procedure used for the preparation of (2S,1R)-2-ethoxy-3-(4-{1-[2-(4-phenoxy-phenyl)-ethylcarbamoyl]-ethoxy}-phenyl)-propionic acid (Example 1, step 3) to produce a colorless oil. MS (ES) for C22H25NO7 [M+H]+: 416.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220880B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-3f93de10e76d4b98b8eac08e1823373f |
| Source note | uspto-grants-2007_05 |