HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 21101710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Reactant | 7-Chloro-4-(piperazin-1-yl)quinoline | HCID 738389 | — |
| Reactant | 2,3-Dihydro-1,4-benzodioxin-5-amine | HCID 11788387 | — |
| Product | HCID 21101710 | HCID 21101710 | — |
Reaction Steps
As described for example 78, 5-amino-1,4-benzodioxane, p-nitrophenyl chloroformate, diisopropylethyl amine, and 7-chloro-4-piperazinylquinoline are reacted to afford the product. LC-MS: 425 (M++1). 1H NMR (DMSO-d6) δ 8.70 (d, 1H), 8.50 (s, 1H), 8.05 (d, 1H), 7.95 (s, 1H), 7.55 (d, 1H), 7.00 (m, 2H), 6.85 (d, 1H), 6.70 (d, 1H), 4.15 (m, 4H), 3.65 (m, 4H), 3.20 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220856B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-9e63c2b61166442885e82b494cc29897 |
| Source note | uspto-grants-2007_05 |