HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22480042, compound → HCID 22480251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22480042 | HCID 22480042 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22480251 | HCID 22480251 | — |
Reaction Steps
The title compound was prepared using methyl 4-[N-(1-perhydro-2H-pyran-2-yl-3-(4-pyridyl)-1H-indazol-5-yl)carbamoyl]benzoate (0.158 g, 035 mmol) as a solution in tetrahydrofuran (3 mL) and 6.0 N aqueous HCl (5 mL). The intermediate was isolated and used without further purification (0.129 g, quantitative): ES-MS (m/z) 373 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07220771B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-fffa7044c4c84fa9a90bfcf64cefd708 |
| Source note | uspto-grants-2007_05 |