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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1353671Generated: October 31, 2026

HCID 22480042, compound → HCID 22480251, compound

https://huagongshe.com/reaction/1353671

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22480042HCID 22480042—
SolventHydrochloric AcidHCID 313—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22480251HCID 22480251—

Reaction Steps

The title compound was prepared using methyl 4-[N-(1-perhydro-2H-pyran-2-yl-3-(4-pyridyl)-1H-indazol-5-yl)carbamoyl]benzoate (0.158 g, 035 mmol) as a solution in tetrahydrofuran (3 mL) and 6.0 N aqueous HCl (5 mL). The intermediate was isolated and used without further purification (0.129 g, quantitative): ES-MS (m/z) 373 [M+1]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07220771B2
Source datasetuspto-grants-2007_05
ORD IDord-fffa7044c4c84fa9a90bfcf64cefd708
Source noteuspto-grants-2007_05