1-(2,3-Dichlorophenyl)piperazine → 3-{4-[4-(2,3-Dichlorophenyl)piperazin-1-yl]butyl}-1H-indole, hydrochloride

Participants

Reaction Steps

from 1-(2,3-dichlorophenyl)piperazine and 3-(4-bromobutyl)-1H-indole. Mp 121–122° C. 1H NMR (DMSO-d6): 1.45–1.55 (m, 2H); 1.65–1.75 (m, 2H); 2.35 (t, 2H); 2.50 (b s, 4H); 2.70 (t, 2H); 2.95 (b s, 4H); 6.95 (t, 1H); 7.05 (t, 1H); 7.10–7.15 (m, 2H); 7.25–7.30 (m, 2H); 7.35 (d, 1H); 7.50 (d, 1H); 10.75 (b s, 1H). Ms m/z: 402 (MH+).

Provenance & Evidence