Octylamine → HCID 21103276, compound

HRID 1354084Notes

Reaction equation

[CH2:1]([NH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].C([O:12][C:13]([CH2:15][N:16]([S:24]([C:27]1[CH:32]=[CH:31][C:30]([N+:33]([O-:35])=[O:34])=[CH:29][CH:28]=1)(=[O:26])=[O:25])[CH:17]([CH2:22]O)[C:18]([O:20][CH3:21])=[O:19])=O)C>>[N+:33]([C:30]1[CH:31]=[CH:32][C:27]([S:24]([N:16]2[CH2:15][C:13](=[O:12])[N:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH2:22][CH:17]2[C:18]([O:20][CH3:21])=[O:19])(=[O:26])=[O:25])=[CH:28][CH:29]=1)([O-:35])=[O:34]

Participants

Reactant 2

HCID 8143Octylamine

HCID 21103279HCID 21103279, compound

Product 1

HCID 21103276HCID 21103276, compoundYield 88%

Procedure

A title compound was prepared by the same method as in Example 31, except that octylamine as the primary amine and the compound of Example 55 were used to obtain a white solid title compound (yield 88%).

Sources & evidence

ORD record: ord-e118bf7c6c254e7894c98feadde78ac2
Source dataset: uspto-grants-2007_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07223751B2

Reaction notes

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