Methanol → HCID 21104869, compound

Participants

Reaction Steps

The above compound (6) (88 mg) was dissolved in methanol (12 mL) and 10% Pd—C (20 mg) was added, and the mixture was stirred under a hydrogen atmosphere at room temperature for 2 hours. After the catalyst was removed by filtration and the filtrate was concentrated under reduced pressure, the resulting residue was freeze-dried to obtain the titled compound (60 mg) as a colorless amorphous.

Provenance & Evidence