Methanol → HCID 21104870, compound

Participants

Reaction Conditions

Reaction Steps

The above compound (6) (1.68 g) was dissolved in methanol (70 mL) and 10% Pd—C (350 mg) was added, and then the mixture was stirred under a hydrogen atmosphere at 40° C. for 2 hours. The catalyst was removed by filtration and the filtrate was concentrated under reduced pressure. The resulting residue was purified by silica gel medium pressure column chromatography (chloroform:methanol=20:1→9:1. 4:1) to obtain the titled compound (951 mg) as a colorless powder.

Provenance & Evidence