4,4'-Dimethoxybenzoin → HCID 178489020, compound

HRID 1354342Notes

Reaction equation

HRID 1354342 reaction equation
[C:1]1([C:9]([CH:11]([C:13]2[CH:20]=[CH:19][C:16]([O:17][CH3:18])=[CH:15][CH:14]=2)O)=O)[CH:8]=[CH:7][C:4]([O:5][CH3:6])=[CH:3][CH:2]=1.[CH3:21][NH:22][C:23]([NH2:25])=[S:24]>>[CH3:6][O:5][C:4]1[CH:7]=[CH:8][C:1]([C:9]2[N:25]=[C:23]([SH:24])[N:22]([CH3:21])[C:11]=2[C:13]2[CH:20]=[CH:19][C:16]([O:17][CH3:18])=[CH:15][CH:14]=2)=[CH:2][CH:3]=1

Participants

3

Reactant 2

HCID 954154,4'-DimethoxybenzoinHCID 2723704Methylthiourea

Product 1

HCID 178489020HCID 178489020, compound

Procedure

13.6 g (50 mmol) of p-anisoin and 6.8 g (75 mmol) of N-methylthiourea were reacted as in example 10. The yield was 7.4 g.

Sources & evidence

ORD record
ord-461146438bf74c5d94ae5c264f056fad
Source dataset
uspto-grants-2007_05
Patent number
US07223781B2

Reaction notes

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