Water → HCID 91268970, compound

Participants

Reaction Steps

To a solution of the product from Example 4 step (a) (92 mg) in THF (5 ml) was added sodium hydride (60% in oil; 10 mg) followed by iodomethane (60 μl). The mixture was stirred at room temperature for 2 days then poured into water and extracted with diethyl ether (three times). The combined organic layers were washed with brine and dried (MgSO4). The solvent was evaporated off to give the sub-title compound (100 mg) as an oil.

Provenance & Evidence