Oxalyl chloride → 2-Chlorobenzoyl isocyanate

Participants

Reaction Steps

1.03 g (6.6 mmol) of 2-chlorobenzamide were suspended in 3 ml of dichloromethane. After 1.17 g (9.2 mmol) of oxalyl chloride had been added, the mixture was heated to reflux for 17 hours. The reaction mixture was then concentrated under high vacuum and reacted in step b without any further purification.

Provenance & Evidence