HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 21105559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 3-(N-Acetyl-N-ethylamino)pyrrolidine | HCID 2756274 | — |
| Reactant | 4-(cyclopentyloxy)aniline | HCID 6484448 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 21105559 | HCID 21105559 | — |
Reaction Steps
N-Ethyl-N-pyrrolidin-3-ylacetamide was reacted with 4-fluoronitrobenzene, the resulting nitro compound was reduced with hydrogen and finally the aniline was reacted with CDI and 4-cyclopentyloxyaniline by method A, B and C. This resulted in the product with the molecular weight of 450.59 (C26H34N4O3); MS (ESI): 451 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07223788B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-0198084755bc4a60b81e757f2605eb82 |
| Source note | uspto-grants-2007_05 |