Methyl iodide → HCID 21105630, compound

HRID 1354680Notes

Reaction equation

HRID 1354680 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH2:13][CH:12]([NH:14][C:15](=[O:17])[CH3:16])[CH2:11]2)=[CH:6][CH:5]=1)([O-:3])=[O:2].I[CH3:19]>>[CH3:19][N:14]([CH:12]1[CH2:11][N:10]([C:7]2[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=2)[CH2:13]1)[C:15](=[O:17])[CH3:16]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 21105567HCID 21105567, compound

Product 1

HCID 21105630HCID 21105630, compound

Procedure

N-[1-(4-nitrophenyl)azetidin-3-yl]acetamide was alkylated with iodomethane by method F. This resulted in the product with the molecular weight of 249.27 (C12H15N3O3); MS (ESI): 250 (M+H+).

Workup

  1. customThis resulted in the product with the molecular weight of 249.27 (C12H15N3O3)

Sources & evidence

ORD record
ord-ab3d42e43a8645ad961ccd259931777e
Source dataset
uspto-grants-2007_05
Patent number
US07223788B2

Reaction notes

Loading…