Methyl iodide → HCID 86594869, compound

HRID 1354685Notes

Reaction equation

HRID 1354685 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH2:13][CH:12]([NH:14][C:15](=[O:21])[O:16][C:17]([CH3:20])([CH3:19])[CH3:18])[CH2:11]2)=[CH:6][CH:5]=1)([O-:3])=[O:2].I[CH3:23]>>[CH3:23][N:14]([CH:12]1[CH2:13][N:10]([C:7]2[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=2)[CH2:11]1)[C:15](=[O:21])[O:16][C:17]([CH3:18])([CH3:20])[CH3:19]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 86594866HCID 86594866, compound

Product 1

HCID 86594869HCID 86594869, compound

Procedure

tert-Butyl [1-(4-nitrophenyl)azetidin-3-yl]carbamate was alkylated with iodomethane by method F. This resulted in the product with the molecular weight of 307.35 (C15H21N3O4); MS (ESI): 308 (M+H+).

Workup

  1. customThis resulted in the product with the molecular weight of 307.35 (C15H21N3O4)

Sources & evidence

ORD record
ord-34218e98e2f7422faf9c6a04f6ea15ba
Source dataset
uspto-grants-2007_05
Patent number
US07223788B2

Reaction notes

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