huagongshe.com
HRID1354709

反应详情

EQUATION

反应方程式

HRID 1354709 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：CNC1CCN(c2ccc(N(C)C(=O)c3ccc(C4CCCCC4)cc3)cc2)C1=O
HCID21105490

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)CNC1CCN(c2ccc(N(C)C(=O)c3ccc(C4CCCCC4)cc3)cc2)C1=O
HCID21105570

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

4-Cyclohexyl-N-methyl-N-[4-(3-methylamino-2-oxopyrrolidin-1-yl)phenyl]benzamide (52 mg) was mixed with pyridine (0.5 ml) and acetic anhydride (130 mg) and, after 3 hours, volatile fractions were removed in vacuo. This resulted in the product with the molecular weight of 447.58 (C27H33N3O3); MS (ESI): 448 (M+H+).

WORKUP

后处理

  1. customvolatile fractions were removed in vacuo
  2. customThis resulted in the product with the molecular weight of 447.58 (C27H33N3O3)