HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzamide → N-1-Naphthylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzamide | HCID 2331 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | HCID 1796834 | HCID 1796834 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-1-Naphthylbenzamide | HCID 69448 | 95% |
Reaction Steps
Following the general procedure, 1-naphthyl tosylate (149 mg, 0.5 mmol) was coupled with benzamide (90 mg, 0.75 mmol) with the reaction time of 20 h. Chromatography on silica gel column with 4:1 hexane:ethyl acetate gave 117 mg (95%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07223879B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-1e653f37333641c18514bdf8639e2612 |
| Source note | uspto-grants-2007_05 |