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Glycerol → N,N-dibutylethanolamine glycerol borate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Glycerol | HCID 753 | — |
| 反応物 | 2-(Dibutylamino)ethanol | HCID 7621 | — |
| 反応物 | Boric Acid | HCID 7628 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N,N-dibutylethanolamine glycerol borate | HCID 131723940 | 87.6% |
反応手順
N,N-dibutylethanolamine/glycerol borate was prepared as follows. Boric acid (10.3 grams), glycerol (15.3 grams), and N,N-dibutylethanolamine (28.9 grams) were added to a 250 milliliter flask. One hundred fifty milliliters of toluene was then added. The reaction was allowed to proceed overnight at 110° C., and the byproduct water (˜9 grams) was continuously removed from the reaction by azeotropic distillation. The final solution was evaporated to remove toluene under vacuum, and a brownish viscous liquid product (˜45 grams) of N,N-dibutylethanolamine/glycerol borate was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06585816B1 |
| 出典データセット | uspto-grants-2003_07 |
| ORD ID | ord-1511e687fae749029932d3f9af5f4682 |
| 出典メモ | uspto-grants-2003_07 |