HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl methyl sulfide → 2-Amino-4-(2-methylsulfanyl-ethylsulfanyl)-6-phenyl-pyrimidine-5-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl methyl sulfide | HCID 10965 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 178509378 | HCID 178509378 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Amino-4-(2-methylsulfanyl-ethylsulfanyl)-6-phenyl-pyrimidine-5-carbonitrile | HCID 18507508 | — |
Reaction Steps
From 2-amino-4-phenyl-6-thioxo-1,6-dihydro-pyrimidine-5-carbonitrile, 2-chloroethyl methylsulfide and sodium ethylate in ethanol. EI-MS m/e (%): 302 (M+, 2), 228 ([M—MeSCH═CH2]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-952b472183f245cb889c4736f5e1f415 |
| Source note | uspto-grants-2003_07 |