1-Benzoylpiperazine → HCID 18507594, compound

HRID 1355814Notes

Reaction equation

HRID 1355814 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4](S(C)(=O)=O)[N:3]=1.[C:19]1([C:25]([N:27]2[CH2:32][CH2:31][NH:30][CH2:29][CH2:28]2)=[O:26])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>COCCOC>[NH2:1][C:2]1[N:3]=[C:4]([N:30]2[CH2:31][CH2:32][N:27]([C:25](=[O:26])[C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH2:28][CH2:29]2)[C:5]([C:13]#[N:14])=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[N:7]=1

Participants

4

Reactant 2

HCID 7626541-BenzoylpiperazineHCID 185073992-Amino-4-furan-2-yl-6-methanesulfonyl-pyrimidine-5-carbonitrile

Product 1

HCID 18507594HCID 18507594, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-furan-2-yl-6-methanesulfonyl-pyrimidine-5-carbonitrile and phenyl-piperazin-1-ylmethanone in DME. ES-MS m/e (%): 397 (M+Na+, 25),375 (M+H+, 100).

Sources & evidence

ORD record
ord-886578fb880c4dc68400fbc9a36df865
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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