1,2-Ethanediamine, N1-phenyl- → HCID 18507493, compound

HRID 1355853Notes

Reaction equation

HRID 1355853 reaction equation
[Br:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[C:17]1([NH:23][CH2:24][CH2:25][NH2:26])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>O1CCOCC1>[Br:1][C:2]1[C:7]([NH:26][CH2:25][CH2:24][NH:23][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[N:6][C:5]([NH2:11])=[N:4][C:3]=1[C:12]1[O:13][CH:14]=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 742701,2-Ethanediamine, N1-phenyl-HCID 185072865-Bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine

Product 1

HCID 18507493HCID 18507493, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine and N-phenylethylenediamine in dioxane. ES-MS m/e (%): 376 (M{81Br}+H+, 100), 374 (M{79Br}+H+, 95).

Sources & evidence

ORD record
ord-c195049b6f264effabfaf7a075ed8271
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

Loading…