1,2-Ethanediamine, N1-phenyl- → HCID 18507364, compound

HRID 1355857Notes

Reaction equation

HRID 1355857 reaction equation
[Cl:1][C:2]1[C:3]([C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:4][C:5]([NH2:11])=[N:6][C:7]=1S(C)=O.[C:17]1([NH:23][CH2:24][CH2:25][NH2:26])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>COCCOC>[Cl:1][C:2]1[C:7]([NH:26][CH2:25][CH2:24][NH:23][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[N:6][C:5]([NH2:11])=[N:4][C:3]=1[C:12]1[O:13][CH:14]=[CH:15][CH:16]=1

Participants

4

Reactant 2

HCID 742701,2-Ethanediamine, N1-phenyl-HCID 18507343HCID 18507343, compound

Product 1

HCID 18507364HCID 18507364, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 5-chloro-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine and N-phenylethylenediamine in DME. ES-MS m/e (%): 332 (M{37Cl}+H+, 40), 330 (M{35Cl}+H+, 100).

Sources & evidence

ORD record
ord-3746d46eebed4521907fe56ca130ef53
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

Loading…