1,2-Ethanediamine, N1-phenyl- → HCID 18507496, compound

HRID 1355859Notes

Reaction equation

HRID 1355859 reaction equation
[NH2:1][C:2]1[N:7]=[C:6](OS(C(F)(F)F)(=O)=O)[C:5]([N+:16]([O-:18])=[O:17])=[C:4]([C:19]2[O:20][CH:21]=[CH:22][CH:23]=2)[N:3]=1.[C:24]1([NH:30][CH2:31][CH2:32][NH2:33])[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>COCCOC>[O:20]1[CH:21]=[CH:22][CH:23]=[C:19]1[C:4]1[N:3]=[C:2]([NH2:1])[N:7]=[C:6]([NH:33][CH2:32][CH2:31][NH:30][C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[C:5]=1[N+:16]([O-:18])=[O:17]

Participants

4

Reactant 2

HCID 742701,2-Ethanediamine, N1-phenyl-HCID 86583748Trifluoromethanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester

Product 1

HCID 18507496HCID 18507496, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From trifluoro-methanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester and N-phenylethylenediamine in DME. ES-MS m/e (%): 363 (M+Na+, 20), 341 (M+H+, 100).

Sources & evidence

ORD record
ord-463d893794dc494fad372879624135f1
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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