1,2-Ethanediamine, N1-phenyl- → HCID 18507268, compound

HRID 1355865Notes

Reaction equation

HRID 1355865 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[C:11]([I:12])=[C:10](S(C)=O)[N:9]=[C:8]([NH2:16])[N:7]=1.[C:17]1([NH:23][CH2:24][CH2:25][NH2:26])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>O1CCOCC1>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[N:7]=[C:8]([NH2:16])[N:9]=[C:10]([NH:26][CH2:25][CH2:24][NH:23][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[C:11]=1[I:12]

Participants

4

Reactant 2

HCID 742701,2-Ethanediamine, N1-phenyl-HCID 18507211HCID 18507211, compound

Product 1

HCID 18507268HCID 18507268, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

From 4-furan-2-yl-5-iodo-6-methanesulfinyl-pyrimidin-2-yl-amine and N-phenylethylenediamine in dioxane. ES-MS m/e (%): 422 (M+H+, 100).

Sources & evidence

ORD record
ord-a7f32501a9874781a34af7e1e77f4020
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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