1,2-Ethanediamine, N1-phenyl- → HCID 18507405, compound

HRID 1355880Notes

Reaction equation

HRID 1355880 reaction equation
[NH2:1][C:2]1[N:7]=[C:6](S(C)=O)[C:5]([C:11]#[N:12])=[C:4]([C:13]2[S:14][CH:15]=[CH:16][CH:17]=2)[N:3]=1.[C:18]1([NH:24][CH2:25][CH2:26][NH2:27])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>O1CCOCC1>[NH2:1][C:2]1[N:7]=[C:6]([NH:27][CH2:26][CH2:25][NH:24][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:5]([C:11]#[N:12])=[C:4]([C:13]2[S:14][CH:15]=[CH:16][CH:17]=2)[N:3]=1

Participants

4

Reactant 2

HCID 742701,2-Ethanediamine, N1-phenyl-HCID 18507414HCID 18507414, compound

Product 1

HCID 18507405HCID 18507405, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

From 2-amino-4-methanesulfinyl-6-thiophen-2-yl-pyrimidine-5-carbonitrile and N-phenylethylenediamine in dioxane. ES-MS m/e (%): 337 (M+H+, 100).

Sources & evidence

ORD record
ord-c1556605d70645b89912b59b688ad921
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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