HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 18507469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 5-Bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine | HCID 18507286 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18507469 | HCID 18507469 | — |
Reaction Steps
From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine, thiophenol and DBU in dioxane. EI-MS m/e (%): 349 (M{81Br}+, 40), 348 ([M{81Br}-H]+, 28), 347 (M{79Br}+, 39), 346 ([M{79Br}-H]+, 24), 268 ([M—Br]+, 100), 175 (92).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-a49202af6331445abfcaaf9e860f2f8b |
| Source note | uspto-grants-2003_07 |