HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 5-Bromo-4-furan-2-yl-6-phenoxy-pyrimidin-2-yl-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 5-Bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-ylamine | HCID 18507286 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 5-Bromo-4-furan-2-yl-6-phenoxy-pyrimidin-2-yl-amine | HCID 18507574 | — |
Reaction Steps
From 5-bromo-4-furan-2-yl-6-methanesulfinyl-pyrimidin-2-yl-amine, phenol and DBU in dioxane. EI-MS m/e (%): 333 (M{81Br}+, 64), 331 (M{79Br}+, 68), 252 ([M—Br]+, 100), 159 (98).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-9632e8cb98224852bc37013f6e0e0538 |
| Source note | uspto-grants-2003_07 |