2-(Benzenesulfonyl)-3-phenyloxaziridine → HCID 18507288, compound

Participants

Reaction Steps

To a stirred suspension of 680 mg (2.66 mmol) 2-amino-4-furan-2-yl-6-methylsulfanyl-pyridine-3,5-dicarbonitrile in 25 ml dichloromethane was added 1,39 g (5.32 mmol) 3!phenyl-2-(phenylsulfonyl)oxaziridine and stirring continued for 48 hours at room temperature. The resulting crystals were collected by filtration and washed with cold dichloromethane to afford 670 mg (93%) 2-amino-4-furan-2-yl-6-methanesulfinyl-pyridine-3,5-dicarbonitrile as a light brown crystalline solid. ES-MS m/e (%): 295 (M+Na+, 70), 273 (M+H+, 100).

Provenance & Evidence