HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → 4-Benzyloxy-6-furan-2-yl-5-nitro-pyrimidin-2-yl-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | Trifluoromethanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester | HCID 86583748 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 4-Benzyloxy-6-furan-2-yl-5-nitro-pyrimidin-2-yl-amine | HCID 9944577 | — |
Reaction Steps
From trifluoromethanesulfonic acid 2-amino-6-furan-2-yl-5-nitro-pyrimidin-4-yl ester, benzyl alcohol and DBU in DME. ES-MS m/e (%): 313 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-3d4173b792334024b59a74aa9c75893e |
| Source note | uspto-grants-2003_07 |