N-(2,6-dimethylphenyl)-ethylenediamine → HCID 18507380, compound

HRID 1355980Notes

Reaction equation

HRID 1355980 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4](S(C)=O)[N:3]=1.[C:18]1([NH:26][CH2:27][CH2:28][NH2:29])[C:23]([CH3:24])=[CH:22][CH:21]=[CH:20][C:19]=1[CH3:25]>COCCOC>[NH2:1][C:2]1[N:3]=[C:4]([NH:29][CH2:28][CH2:27][NH:26][C:18]2[C:23]([CH3:24])=[CH:22][CH:21]=[CH:20][C:19]=2[CH3:25])[C:5]([C:13]#[N:14])=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[N:7]=1

Participants

4

Reactant 2

HCID 12666312N-(2,6-dimethylphenyl)-ethylenediamineHCID 185076922-Amino-4-(furan-2-YL)-6-(methylsulfinyl)pyrimidine-5-carbonitrile

Product 1

HCID 18507380HCID 18507380, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-furan-2-yl-6-methanesulfinyl-pyrimidine-5-carbonitrile and N-(2,6-xylyl)ethylenediamine in DME. ES-MS m/e (%): 349 (M+H+, 100), 228 ([M+H—C8H11N]+, 65).

Sources & evidence

ORD record
ord-69015a50b23d4d93bee72e4b023b3fb3
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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