2-(2-Aminoethylamino)-5-nitropyridine → HCID 18507634, compound

HRID 1355985Notes

Reaction equation

HRID 1355985 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4](S(C)=O)[N:3]=1.[NH2:18][CH2:19][CH2:20][NH:21][C:22]1[CH:27]=[CH:26][C:25]([N+:28]([O-:30])=[O:29])=[CH:24][N:23]=1>COCCOC>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4]([NH:18][CH2:19][CH2:20][NH:21][C:22]2[CH:27]=[CH:26][C:25]([N+:28]([O-:30])=[O:29])=[CH:24][N:23]=2)[N:3]=1

Participants

4

Reactant 2

HCID 1224252-(2-Aminoethylamino)-5-nitropyridineHCID 185076922-Amino-4-(furan-2-YL)-6-(methylsulfinyl)pyrimidine-5-carbonitrile

Product 1

HCID 18507634HCID 18507634, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-furan-2-yl-6-methanesulfinyl-pyrimidine-5-carbonitrile and 2-(2-aminoethylamino)-5-nitropyridine in DME. ES-MS m/e (%): 389 (M+Na+, 15), 367 (M+H+, 100).

Sources & evidence

ORD record
ord-76dec1bdbdb54524abe5cedc65fc0382
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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