N-Isopropylethylenediamine → HCID 18507613, compound

HRID 1356000Notes

Reaction equation

HRID 1356000 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4](S(C)=O)[N:3]=1.[CH:18]([NH:21][CH2:22][CH2:23][NH2:24])([CH3:20])[CH3:19]>COCCOC>[NH2:1][C:2]1[N:7]=[C:6]([C:8]2[O:9][CH:10]=[CH:11][CH:12]=2)[C:5]([C:13]#[N:14])=[C:4]([NH:24][CH2:23][CH2:22][NH:21][CH:18]([CH3:20])[CH3:19])[N:3]=1

Participants

4

Reactant 2

HCID 88098N-IsopropylethylenediamineHCID 185076922-Amino-4-(furan-2-YL)-6-(methylsulfinyl)pyrimidine-5-carbonitrile

Product 1

HCID 18507613HCID 18507613, compound

Reagents, catalysts & solvents 1

HCID 80711,2-DimethoxyethaneSolvent

Procedure

From 2-amino-4-furan-2-yl-6-methanesulfinyl-pyrimidine-5-carbonitrile and N-isopropylethylenediamine in DME. ES-MS m/e (%): 287 (M+H+, 100), 228 ([M+H-iPrNH2]+, 40).

Sources & evidence

ORD record
ord-37b75cb4217c43a489c1ae204ea5719f
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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