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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1356032Generated: November 1, 2026

1,8-Diazabicyclo(5.4.0)undec-7-ene → HCID 9836197, compound

https://huagongshe.com/reaction/1356032

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,8-Diazabicyclo(5.4.0)undec-7-eneHCID 81184—
Reactant(5-Methylpyridin-2-yl)methanolHCID 12325387—
Reactant2-Amino-4-(furan-2-YL)-6-(methylsulfinyl)pyrimidine-5-carbonitrileHCID 18507692—
Solvent1,2-DimethoxyethaneHCID 8071—
ProductHCID 9836197HCID 9836197—

Reaction Steps

From 2-amino-4-furan-2-yl-6-methanesulfinyl-pyrimidine-5-carbonitrile, (5-methyl-pyridin-2-yl)methanol and DBU in DME. EI-MS m/e (%): 307 (M+, 76), 290 (28), 278 (16), 122 (100), 106 (78), 79 (30), 77 (38).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06586441B2
Source datasetuspto-grants-2003_07
ORD IDord-03a3a89c8dec48c991b25eed0053310c
Source noteuspto-grants-2003_07