HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → 2-Amino-4-benzyloxy-6-chloro-pyrimidine-5-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 2-Amino-4-chloro-6-methanesulfinyl-pyrimidine-5-carbonitrile | HCID 18507277 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 2-Amino-4-benzyloxy-6-chloro-pyrimidine-5-carbonitrile | HCID 18507216 | — |
Reaction Steps
From 2-amino-4-chloro-6-methanesulfinyl-pyrimidine-5-carbonitrile, benzyl alcohol and DBU in DME. EI-MS m/e (%): 262 (M{37Cl}+, 22), 260 (M{35Cl}+,60), 91 (100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586441B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-35cb7a6ccbc344d0ab62a9a0491b4d79 |
| Source note | uspto-grants-2003_07 |