HRID13563

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6569

Methyl ethyl ketone

C4H8O

HCID9351

Hydralazine hydrochloride

C8H9ClN4

PRODUCTS

生成物

HCID22502148

未命名化合物

收率 78%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID22242641

Methanol--water (1/1)

CH6O2

PROCEDURE

实验过程

A 10 parts 1-hydrazinophthalazine HCL (0.05 Molar) in 50% methanol-water are mixed with 1 part 2-butanone. After evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone is crystallized from ethanol-heptane (78% yield). [The Journal of Pharmacology and Experimental Therapeutics 205 (2): 418-425 (1978)].

WORKUP

后处理

customAfter evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone