1-Methoxy-2-propanol → HCID 123358603, compound
Reaction equation
[CH2:1]([Si:9](OC)(OC)OC)[CH2:2][CH2:3][CH2:4][CH2:5][CH:6]([CH3:8])[CH3:7].COCC(O)C>>[CH2:1]([SiH3:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH:6]([CH3:8])[CH3:7]Participants
3
Procedure
Silica nanoparticles surface modified with isooctyltrimethoxysilane were prepared as follows: 61.42 g BS1316 isooctyltrimethoxysilane (Wacker Silicones Corp., Adrian, Mich.), 1940 g 1-methoxy-2-propanol and 1000 g NALCO 2326 colloidal silica were combined in a 1 gallon glass jar. The mixture was shaken to ensure mixing and then placed in an oven at 80° C. overnight. The mixture was then dried in a flow through oven at 150° C. to produce a white particulate solid.
Workup
- customwere prepared
- additionto ensure mixing
- customThe mixture was then dried in a flow through oven at 150° C.
- customto produce a white particulate solid
Sources & evidence
- ORD record
- ord-eb1acf074ca04978b6b996d43840e5da
- Source dataset
- uspto-grants-2003_07
- Patent number
- US06586483B2
Reaction notes
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