HRID13564

反应详情

EQUATION

反应方程式

HRID 13564 的结构方程式

PROCEDURE

实验过程

1-hydrazinophthalazine HCL (395 mg; 2 mmoles) is dissolved in 2.5 ml of acetone and allowed to react for 1 hour. The solvent is evaporated and the slightly yellow material is dried in vacuo to yield 411 mg of 1-hydrazinophthalazine acetone hydrazone. (99% of theoretical yield). [British Journal of Pharmacology 61: 345-349 (1977)]

WORKUP

后处理

  1. customto react for 1 hour
  2. customThe solvent is evaporated
  3. customthe slightly yellow material is dried in vacuo