Methanol → HCID 178498304, compound

HRID 1356443Notes

Reaction equation

HRID 1356443 reaction equation
S(Cl)(Cl)=O.[OH:5][C:6]1[CH:14]=[CH:13][C:9]([C:10]([OH:12])=[O:11])=[CH:8][N:7]=1.[CH3:15]O>>[OH:5][C:6]1[CH:14]=[CH:13][C:9]([C:10]([O:12][CH3:15])=[O:11])=[CH:8][N:7]=1

Participants

4

Reactant 3

HCID 887MethanolHCID 24386Thionyl ChlorideHCID 178418479HCID 178418479, compound

Product 1

HCID 178498304HCID 178498304, compound

Procedure

To methanol (100 ml) in an ice bath was added thionyl chloride (16 ml) followed by addition of 6-hydroxynicotinic acid (10 g).

Sources & evidence

ORD record
ord-ed51b9a26984407d8014ae4f0d85fbd2
Source dataset
uspto-grants-2003_07
Patent number
US06586475B1

Reaction notes

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