HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylparaben → Methyl 4-(pyridin-2-ylmethoxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | 4-Hydroxymethylpyridine | HCID 11472 | — |
| Reactant | 3-(Dimethylamino)-1-propanol | HCID 76646 | — |
| Product | Methyl 4-(pyridin-2-ylmethoxy)benzoate | HCID 2416604 | — |
Reaction Steps
Following the procedure of Example 76(a) except substituting methyl 3-hydroxybenzoate for methyl 4-hydroxybenzoate and 4-pyridylcarbinol for 3-dimethylamino-1-propanol, the title compound was prepared as a yellow solid (0.599 g, 2.5 mmol). MS(ESI): 244.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586466B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-6c26ffd046bf441596fa4b0c48309fe8 |
| Source note | uspto-grants-2003_07 |