HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 86759057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | HCID 18509491 | HCID 18509491 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 86759057 | HCID 86759057 | 42.8% |
Reaction Steps
The procedure described in Example 17 was repeated, except that Compound 36 (2.35 g; 7.3 mmol), n-butyl lithium in n-hexane (1.56 M: 5.2 ml; 8.1 mmol), and acetone (1 ml) were used, to thereby yield 940 mg of the target compound (yield: 42.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586633B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-ae788f5d571746cbb49187f7cd7a52a2 |
| Source note | uspto-grants-2003_07 |