HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Carbonate → HCID 18509427, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 3'-(N-Ethylaminomethyl)acetophenone | HCID 18509490 | — |
| Edukt | 1-Bromo-6,6-dimethylhept-2-en-4-yne | HCID 45489594 | — |
| Produkt | HCID 18509427 | HCID 18509427 | 62,5% |
Reaktionsschritte
The procedure described in Example 13 was repeated, except that 3′-(N-ethylaminomethyl)acetophenone (1.24 g; 7 mmol), sodium carbonate (instead of potassium carbonate) (745 mg; 7 mmol), and 1-bromo-6,6-dimethyl-2-hepten-4-yn (1.41 g; 7 mmol) were used, to thereby yield 1.30 g of the target compound (yield: 62.5%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06586633B1 |
| Quelldatensatz | uspto-grants-2003_07 |
| ORD ID | ord-362400ab657a43f0b66e2b09aeca1b2a |
| Quellennotiz | uspto-grants-2003_07 |