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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1356820Erstellt: 25. Oktober 2026

Sodium Carbonate → HCID 18509427, Verbindung

https://huagongshe.com/reaction/1356820

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktSodium CarbonateHCID 10340—
EduktPotassium CarbonateHCID 11430—
Edukt3'-(N-Ethylaminomethyl)acetophenoneHCID 18509490—
Edukt1-Bromo-6,6-dimethylhept-2-en-4-yneHCID 45489594—
ProduktHCID 18509427HCID 1850942762,5%

Reaktionsschritte

The procedure described in Example 13 was repeated, except that 3′-(N-ethylaminomethyl)acetophenone (1.24 g; 7 mmol), sodium carbonate (instead of potassium carbonate) (745 mg; 7 mmol), and 1-bromo-6,6-dimethyl-2-hepten-4-yn (1.41 g; 7 mmol) were used, to thereby yield 1.30 g of the target compound (yield: 62.5%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06586633B1
Quelldatensatzuspto-grants-2003_07
ORD IDord-362400ab657a43f0b66e2b09aeca1b2a
Quellennotizuspto-grants-2003_07