HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → 3'-(N-Cinnamyl-N-methylaminomethyl)acetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-methyl-3-phenylprop-2-en-1-amine | HCID 189183 | — |
| Reactant | 1-(3-(Bromomethyl)phenyl)ethan-1-one | HCID 15479807 | — |
| Reactant | N,6,6-trimethylhept-2-en-4-yn-1-amine | HCID 53427009 | — |
| Product | 3'-(N-Cinnamyl-N-methylaminomethyl)acetophenone | HCID 69936145 | 49.5% |
Reaction Steps
The procedure described in Example 1 was repeated, except that N-cinnamyl methylamine [instead of N-(6,6-dimethyl-2-hepten-4-ynyl)methylamine] (650 mg; 3.04 mmol), sodium carbonate (instead of potassium carbonate) (1.5 eq), and 3′-bromomethylacetophenone (1.5 eq) were used, to thereby yield 0.42 g of the target compound (yield: 49.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06586633B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-d8416139524347bfac9c50fba1398f58 |
| Source note | uspto-grants-2003_07 |