Propionyl chloride → HCID 18504786, compound

HRID 1356996Notes

Reaction equation

HRID 1356996 reaction equation
[C:1]([N:4]([CH2:14]C)[C:5]1[CH:10]=[CH:9][C:8]([N+:11]([O-:13])=[O:12])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[C:16](Cl)(=O)CC>C1C=CC=CC=1>[C:1]([N:4]([CH3:14])[C:5]1[CH:10]=[CH:9][C:8]([N+:11]([O-:13])=[O:12])=[CH:7][CH:6]=1)(=[O:3])[CH2:2][CH3:16]

Participants

4

Reactant 2

HCID 62324Propionyl chlorideHCID 74583Acetamide, N-ethyl-N-(4-nitrophenyl)-

Product 1

HCID 18504786HCID 18504786, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The reaction is carried out using an analogous method to (9a), using N-methyl-4 nitroanilinc (5 g, 32.86 mmol) in benzene (30 ml), treated with propionyl chloride (15 ml). ES+ (M+1) 208.88.

Sources & evidence

ORD record
ord-a051a84c14f84844a8809138e1865f53
Source dataset
uspto-grants-2003_07
Patent number
US06589950B1

Reaction notes

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