HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl 3-amino-3-(3-nitrophenyl)propanoate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3-Amino-3-(3-nitrophenyl)-propionic acid hydrochloride | HCID 2868206 | — |
| Product | Ethyl 3-amino-3-(3-nitrophenyl)propanoate hydrochloride | HCID 16188861 | — |
Reaction Steps
60 g of (1a) were suspended in 660 ml of ethanol, and gaseous HCl was passed in for 1 h. The reaction mixture was then heated under reflux for 4 h and then cooled and concentrated. 62 g of a white solid were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06589972B2 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-bc088d423f3b4394927a13bad3b6a3ba |
| Source note | uspto-grants-2003_07 |