3-Nitrobenzenesulfonyl chloride → HCID 70018028, compound

HRID 1357078Notes

Reaction equation

HRID 1357078 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH2:8][CH:9]([NH:15][C:16](=[O:25])[CH2:17][CH2:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[CH:6][CH:7]=1.[N+:26]([C:29]1[CH:30]=[C:31]([S:35](Cl)(=[O:37])=[O:36])[CH:32]=[CH:33][CH:34]=1)([O-:28])=[O:27]>>[N+:26]([C:29]1[CH:30]=[C:31]([S:35]([NH:1][C:2]2[CH:3]=[C:4]([CH2:8][CH:9]([NH:15][C:16](=[O:25])[CH2:17][CH2:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[CH:6][CH:7]=2)(=[O:37])=[O:36])[CH:32]=[CH:33][CH:34]=1)([O-:28])=[O:27]

Participants

3

Reactant 2

HCID 84763-Nitrobenzenesulfonyl chlorideHCID 70018205HCID 70018205, compound

Product 1

HCID 70018028HCID 70018028, compound

Procedure

Corresponding to Example 3c, 1.2 g of (6b) were reacted with 3-nitrophenylsulphonyl chloride. A solid was obtained (yield: 1.54 g).

Workup

  1. customA solid was obtained (yield: 1.54 g)

Sources & evidence

ORD record
ord-af749442440c4fe58981686eaf7e8522
Source dataset
uspto-grants-2003_07
Patent number
US06589972B2

Reaction notes

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