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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1357132Generated: November 4, 2026

HCID 69596698, compound → HCID 69596721, compound

https://huagongshe.com/reaction/1357132

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69596698HCID 69596698—
SolventChloroformHCID 6212—
ProductHCID 69596721HCID 69596721—

Reaction Steps

The title compound, white solid, m.p. 96° C., [α]D20=−97.1° (c=1.0723 in chloroform) and MS: m/e=378.2 (M+H+)]was prepared in accordance with the general method of example 44 from (2S,5R)-3-[5-(4-fluoro-phenyl)-1-(toluene-4-sulfonyl)-pyrrolidin-2-yl]-propionic acid methyl ester [see example 59: colorless oil, [α]D20=−96.4° (c=1.0992 in chloroform) and MS: m/e=406.1 (M+H+)].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06589978B2
Source datasetuspto-grants-2003_07
ORD IDord-b26da6caaaf2477fbd5154890431a0f7
Source noteuspto-grants-2003_07