Sebacic Acid → Dipotassium sebacate

HRID 1357437Notes

Reaction equation

HRID 1357437 reaction equation
[C:1]([OH:14])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11].[OH-].[K+:16]>O>[C:1]([O-:14])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([O-:12])=[O:11].[K+:16].[K+:16]

Participants

4

Reactant 2

HCID 5192Sebacic AcidHCID 14797Potassium Hydroxide

Product 1

HCID 3016755Dipotassium sebacate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
85 °C

Procedure

Such a salt was prepared through the following procedure: 432 grams of distilled water, 100 grams of Sebacic Acid (available from Arizona Chemical) and 112 grams of 45% KOH (available through Brenntag Southeast distributors) was added to a 1000 ml three neck round bottom flask. The flask was purged with nitrogen and heated to 80-90° C. and held for 2 hours. The acid value of the resulting product was 0.28 mg KOH/gram of sample.

Workup

  1. customSuch a salt was prepared through the following procedure
  2. customThe flask was purged with nitrogen

Sources & evidence

ORD record
ord-fd6796649ffc4a0a9818d2ad9c495a20
Source dataset
uspto-grants-2003_07
Patent number
US06591548B2

Reaction notes

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