HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 70020197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 91573293 | HCID 91573293 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70020197 | HCID 70020197 | 54% |
Reaction Steps
Para-toluenesulfonic acid monohydrate (100 mg, 0.526 mmol) was added to a room temperature solution of Example 13D in methanol (50 mL). After stirring overnight, the reaction mixture was concentrated and the concentrate was purified by flash chromatography using ethyl acetate to afford 0.90 g (54%) of the desired product as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06593314B1 |
| Source dataset | uspto-grants-2003_07 |
| ORD ID | ord-4a8bb7ea683a48aa81c6a55d6a071bbc |
| Source note | uspto-grants-2003_07 |