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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1357502Generated: November 2, 2026

p-Toluenesulfonic acid monohydrate → HCID 70020197, compound

https://huagongshe.com/reaction/1357502

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonic acid monohydrateHCID 521998—
ReactantHCID 91573293HCID 91573293—
SolventMethanolHCID 887—
ProductHCID 70020197HCID 7002019754%

Reaction Steps

Para-toluenesulfonic acid monohydrate (100 mg, 0.526 mmol) was added to a room temperature solution of Example 13D in methanol (50 mL). After stirring overnight, the reaction mixture was concentrated and the concentrate was purified by flash chromatography using ethyl acetate to afford 0.90 g (54%) of the desired product as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06593314B1
Source datasetuspto-grants-2003_07
ORD IDord-4a8bb7ea683a48aa81c6a55d6a071bbc
Source noteuspto-grants-2003_07